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Effects of MgO modified β-TCP nanoparticles on the microstructure and properties of β-TCP/Mg-Zn-Zr composites

机译:MgO修饰的β-TCP纳米颗粒对β-TCP/ Mg-Zn-Zr复合材料微观结构和性能的影响

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摘要

The mechanical properties and corrosion resistance of magnesium alloy composites were improved by the addition of MgO surface modified tricalcium phosphate ceramic nanoparticles (m-β-TCP). Mg-3Zn-0.8Zr composites with unmodified (MZZT) and modified (MZZMT) nanoparticles were produced by high shear mixing technology. Effects of MgO m-β-TCP nanoparticles on the microstructure, mechanical properties, electrochemical corrosion properties and cytocompatibility of Mg-Zn-Zr/β-TCP composites were investigated. After hot extrusion deformation and dynamic recrystallization, the grain size of MZZMT was the half size of MZZT and the distribution of m-β-TCP particles in the matrix was more uniform than β-TCP particles. The yield tensile strength (YTS), ultimate tensile strength (UTS), and corrosion potential (Ecorr) of MZZMT were higher than MZZT; the corrosion current density (Icorr) of MZZMT was lower than MZZT. Cell proliferation of co-cultured MZZMT and MZZT composite samples were roughly the same and the cell number at each time point is higher for MZZMT than for MZZT samples.
机译:通过添加MgO表面改性的磷酸三钙陶瓷纳米粒子(m-β-TCP),可以改善镁合金复合材料的机械性能和耐蚀性。采用高剪切混合技术制备了具有未改性(MZZT)和改性(MZZMT)纳米粒子的Mg-3Zn-0.8Zr复合材料。研究了MgOm-β-TCP纳米颗粒对Mg-Zn-Zr /β-TCP复合材料的微观结构,力学性能,电化学腐蚀性能和细胞相容性的影响。经过热挤压变形和动态重结晶后,MZZMT的晶粒尺寸为MZZT的一半,并且基质中m-β-TCP颗粒的分布比β-TCP颗粒更均匀。 MZZMT的屈服抗拉强度(YTS),极限抗拉强度(UTS)和腐蚀电位(Ecorr)均高于MZZT。 MZZMT的腐蚀电流密度(Icorr)低于MZZT。共培养的MZZMT和MZZT复合样品的细胞增殖大致相同,并且MZZMT在每个时间点的细胞数均高于MZZT样品。

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