N-(m-ferrocenylphenyl)-formamide has been synthesized by the reaction of m-ferrocenyl-aniline with DMF, and characterized by elements analysis, IR, 1H NMR, and X-ray structure determination. The crystallized was in the monoclinic, P21/c space group, with a=0.140 94(3) nm, b=0.102 87(2) nm, c=0.100 26(2) nm, β=104.85(3)°and final R indices [I＞2σ(I)] R1=0.072 7, wR2=0.184 5. An infinite one-dimensional chain is formed by interferrocenylaniline). CCDC: 243511.
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