A device based on a high pressure die-casting(HPDC) machine was constructed,with a capacity to produce thixo-casts from steel.After inductive heating to the required semi-solid temperature range,the samples were transported in a protective argon atmosphere to a cylinder of modified HPDC and injected into a pre-heated die.Bearing steel 100Cr6(after forging) was used as the feedstock material.The metallographic analysis of the steel showed a homogenous structure within a whole volume characterized by a grain size between 2 μm and 8 μm.Differential scanning calorimetry(DSC) analysis allowed to estimate the process temperature for thixoforming at 1 390 ?C which was attributed to about 45% of a liquid phase.With such technological parameters after the semi-solid processing the microstructure consisted of globular grains of size from 15 μm to 40 μm.The microstructure of globules indicated predominant presence of martensite(about 76% volume fraction) with residual austenite between plates.X-ray analysis confirmed that the thixo-cast samples contain mainly martensite and residual austenite.The hardness of the initial forged sample was HRC 27 and after the thixoforming process it was HRC 60,which confirms the presence of martensite and carbides.The thixo-casts were subjected to low tempering,at temperature of 150 °C for a period of 2 h,in order to remove stresses created during the process of thixoforming and to increase plasticity.The hardness after tempering was HRC 62.3.Additionally,in order to identify phases present in the thixo-casts,transmission electron microscopy(TEM) was carried out.
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