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长江油气(英文版)

长江油气(英文版)

《Open Journal of Yangtze Oil and Gas》（长江油气英文版）是由长江大学主办，与科研出版社联合出版发行的，反映国内外石油天然气工业领域高水平学术成果的英文刊物。Open Journal of Yangtze Oil and Gas办刊宗旨是为中外石油科学家搭建一个高水平的学术交流平台，汇集石油地质、物探、开发、机械等方面的研究新发现、新成果。
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    国际刊号/ISSN：2473-1889
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  • 主编：邓运华
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  • 邮箱：ojogas@yangtzeu.edu.cn
  • 地址：中国湖北荆州
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长江油气(英文版) >2023年第2期

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  • 摘要：The Sulige gas field is a typical low-pressure low-permeability tight sandstone gas reservoir. The reservoir has poor seepage capacity, strong heterogeneity, high mineralization of formation water and extremely scarce water resources on the site. These unfavorable factors have brought great difficulties to the on-site mining process. Now, a nano-composite green environmental protection slick water fracturing fluid system CQFR can be quickly dissolved because of the larger specific surface area, and the small molecular size makes the damage to the reservoir less than 5%, and the average drag reduction effect can reach more than 73%. It can quickly and well dissolve and maintain performance under high salinity conditions and fracturing flowback fluids. It responds well to the complex reservoir conditions on the construction site and makes the flowback fluid recyable, which greatly reduces the consumption of water resources on the construction site and effectively improves the construction efficiency and economic benefits.
  • 摘要：Recently, the problem of phenolic organics pollution has become increasingly serious. More and more strategies have been developed to remove phenolic organics from water, including oxidation, adsorption, chemical precipitation, etc. Among them, adsorption technology has attracted great attention due to its advantages of high efficiency, simplicity and easy operation. In this study, the natural shale soil without any modification was directly used as adsorbent to remove phenol from aqueous solutions. The shale soil samples were characterized by scanning electron microscope (SEM), X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR) and nitrogen adsorption-desorption isotherms. Detailed kinetics and isotherm studies of phenol adsorption onto shale were investigated. According to the results of the orthogonal test, the influence degree of the four factors on the removal of phenol by soil samples was operating temperature > adsorbent dosage > contact time > pH. The adsorption kinetics of phenols by the soil corresponded with the pseudo-second-order kinetic model. Thermodynamic studies indicated that Freundlich adsorption isotherm model could better describe phenol removal characteristics than Langmuir adsorption isotherm model. And the maximum adsorption capacity was found to be 9.68 mg/g for phenol. It is concluded that shale soil without any modification or activated methods could be employed as a low-cost alternative adsorbent for wastewater treatment.
  • 摘要：Brownshale is a lithology unit in the middle of the Pematang Formation consisting of brown to black shale that is deposited in the lacustrine environment. Brownshale from the results of previous studies stated as the main source rock in the Central Sumatra Basin, which is spread over several troughs, namely Balam, Aman, Rangau, Kiri, and Bengkalis Troughs, where Bengkalis Trough is the most extensive Trough. In the shale hydrocarbon prospecting analysis, Brownshale from previous researchers concluded that it had good prospects, based on several parameters including: TOC values with poor to very good quality. Brownshale formation is a type of kerogene as kerogen type of II/III, brittleness index greater than 0.48, and rock compressive strength below 10,000 Psi. One method in the development phase of shale hydrocarbon is to determine the fracable sweetspot window using drill cuttings and TOC, because there is no core data available. Based on the results of the well log analysis of well BS-03, it is obtained information that the Brownshale formation has a thickness of 1028 feet with intercalation laminated shale/sand section, so the mineral content varies greatly. From the ternary diagram of XRD (bulk analysis) results of drill cuttings of Brownshale formation of well BS-03, it can be seen that mineral distribution of Quartz-Clay-Calcite (Q-C-C) is spread between zone 1 to zone 3, namely: Dominant Quartz - Minor Clay & Carbonate (Zone 1: Brittle Quartz Rich), Dominant Carbonate - Quartz & Minor Clay (Zone 2: Brittle Carbonate Rich), and Quartz & Carbonate Balance - Clay minor (Zone 3: Ductile, hard to frac). This shows that not all Brownshale formation intervals are easy to frac (high fracability). From the XRD result, percentage of mineral content (bulk analysis) of Brownshale drill cuttings, there is an interesting phenomenon, i.e. the presence of sillimanite and kaliophilite minerals significantly starting at a depth of 10,780 ft and below, where both minerals have tenacity: brittle, and also from the results of the MBT analysis seen an interesting phenomenon, i.e. at a depth interval of about 10,780 ft the value of CEC drops below 3 meq/100 grams, and can be categorized as the brittle shale. Referring to the presence of sillimanite and kaliophilite minerals, as well as low MBT values, then at intervals of 10,780 ft below, it can be seen that at the bottom of the depth interval as a fracable sweetspot window, and at the upper depth interval of the Brownshale formation, it is believed to be a fracture barrier.
  • 摘要：With the enhancement of environmental protection awareness, the requirements on drilling fluid are increasingly strict, and the use of ordinary oil-based drilling fluid has been strictly restricted. In order to solve the environmental protection and oil-gas reservoir protection problems of offshore oil drilling, a new synthetic basic drilling fluid system is developed. The basic formula is as follows: a basic fluid (80% Linear a-olefin + 20% Simulated seawater) + 2.5% nano organobentonite + 3.5% emulsifier RHJ-5# + 2.5% fluid loss agent SDJ-1 + 1.5% CaO + the right amount of oil wetting barite to adjust the density, and a multifunctional oil and gas formation protective agent YRZ has been developed. The performance was evaluated using a high-low-high-temperature rheometer, a high-temperature and high-pressure demulsification voltage tester, and a high-temperature and high-pressure dynamic fluid loss meter. The results show that the developed synthetic based drilling fluid has good rheological property, demulsification voltage ≥ 500 V, temperature resistance up to 160°C, high temperature and high pressure filtration loss < 3.5 mL. After adding 2% - 5% YRZ into the basic formula of synthetic based drilling fluid, the permeability recovery value exceeds 90% and the reservoir protection effect is excellent. The new synthetic deepwater drilling fluid is expected to have a good application prospect in offshore deepwater drilling.
  • 摘要：Fracturing fluid is the blood of fracturing construction, which is very important for fracturing, which requires that fracturing fluid needs to have good performance. The three commonly used fracturing fluids for unconventional oil and gas reservoir transformation are: 1) Guar gum fracturing fluid;2) Water-based emulsion slippery water fracturing fluid;3) Oil-based emulsion slippery water fracturing fluid. In this paper, water samples and other experimental data provided by Mahu Oilfield are used to evaluate three different fracturing fluid systems in laboratory. The formulas of the three different fracturing fluid systems are: 1) Water-based emulsion slippery water fracturing fluid is clean slippery water fracturing fluid 0.1% JHFR-2D drag reducer + 0.2% JHFD-2 multifunctional additive;2) Oil-based emulsion slippery water fracturing fluid 0.1% A agent + 0.2% B agent;3) Guar gum fracturing fluid 0.1% guanidine gum + 0.5% drainage aid + 0.3% demulsifier. The compatibility, drag reduction performance, reservoir damage, residue content, anti-swelling performance, surface interfacial tension, viscosity and other properties of three different slippery water fracturing fluid systems were studied. Through laboratory experiments, the comprehensive indicators show that clean slippery water fracturing fluid has obvious advantages.
  • 摘要：The kinetic characteristics of alkenes involved in thermochemical sulfate reduction (TSR) have been never reported in geological literature. In this study, TSR by ethene under hydrothermal conditions was performed in the constrained simulation experiments. Typical TSR products consisted of H2S, CO2, mercaptans, sulfides, thiophenes derivatives and benzothiophene. The apparent activation energy E and apparent frequency factor A for TSR by ethene were determined as 76.370 kJ/mol and 4.579 s-1, respectively. The lower activation energy for ethene involved in TSR relative to ethane suggested that the reactivity of ethene is much higher than that of ethane, in accordance with the thermodynamic analysis. Rate constants were determined experimentally using first-order kinetics extrapolate to MgSO4 half-lives of 67.329 years - 3.053 years in deep burial diagenetic settings (120°C - 180°C). These values demonstrate that the reaction rate for TSR by ethene is extraordinarily fast in high-temperature gas reservoirs (120°C - 180°C). Consequently, the newly formed ethene from thermal cracking and TSR alteration of natural gas and/or petroleum could not survive after TSR process and were rarely detected in natural TSR reservoirs.
  • 摘要：Kendeng Basin stretches in an E-W direction from the Quaternary Merapi-Ungaran Volcano range in the West to the Madura Strait East of Jawa Timur Province, Indonesia. With Quaternary volcanic deposits covering this basin, its subsurface configuration has not been accurately identified. Several scholars suggest that its configuration forms an asymmetrical basin deepening to the south as a result of volcanic deposits and extending E-W direction. This paper answers what configuration Kendeng Basin has, including whether it consists of a simple asymmetrical shape as previous studies have interpreted or other patterns due to tectonic processes that took place during its formation. The research employed Gravity and Magnetic method, and the results were processed by spectral and gradient analyses. Both analyses revealed that Kendeng Basin formed Horst-Graben structures extending in an E-W direction based on a response to compression and strain forces during its formation. A structure with an E-W direction controls the shape of the Horst-Graben and is transected by a structural pattern extending in a NE-SW direction or known as the Meratus pattern. These findings provide an alternative to the concept of oil and gas exploration, which, until today, is merely known from the emergence of oil seepages in Kendeng Basin.
  • 摘要：Sillimanite is a brittle mineral as a metamorphic mineral product which is generally derived from clay, along with an increase in pressure and high temperature (600°C - 900°C), and kaliophilite is also a brittle mineral as a potassium bearing in the sand-shale series, which contributes to the clay diagenesis process. In the development of shale hydrocarbon in the Brownshale formation in the Bengkalis Trough, Central Sumatra Basin, using the correlation of the XRD (bulk and clay oriented), TOC, Ro, and MBT analysis results from the drill cuttings of well BS-03, so that the fracable zone interval can be determined. From this correlation, it shows that the presence of sillimanite and kaliophilite minerals as minor minerals greatly affects the changes in shale character and hydrocarbon generation, where at depth intervals of 10,780 ft downward (sand series-shale) there is an interesting phenomenon, i.e. low MBT, low TOC, and high Ro, so it is believed that the depth interval of 10,780 ft downward is a fracable zone interval (brittle shale) which is a good candidate for hydraulic fracking planning, while the upper depth interval is a fracture barrier.
  • 摘要：This paper proposed a method of injection-production system adjustment to solve the problem that the water flooding effect was restricted because of the horizontal and vertical contradictions during the development process of fault block reservoirs. Considering the heterogeneity of reservoir, the Buckley-Leverett water flooding theory was applied to establish the relationship between the recovery and cumulative water injection. In order to achieve the goal of vertically balanced recovery of each section, the calculation method of vertical sectional injection allocation was proposed. The planar triangular seepage unit was assumed and sweep coefficients of different oil-water distribution patterns were characterized using multi-flow tube method. In order to balance and maximize the plane sweep coefficient, the calculation method of plane production system optimization was obtained. Then the injection-production system stereoscopic adjustment method based on equilibrium displacement was proposed with vertical sectional injection allocation and plane production system optimization. This method was applied to injection and production adjustment of BZ oilfield in southern Bohai. The effect of water control and oil increase was obvious. This method can greatly improve the effect of water flooding of offshore fault block reservoirs with the adjustment of injection-production system.
  • 摘要：Hydraulic fracturing is among the approaches used to optimize production from a gas condensate reservoir. A detailed economic analysis is required to evaluate the profitability and feasibility of hydraulic fracturing as an optimization option in a gas condensate reservoir operating below dewpoint. The objective of this research is to evaluate the economic benefits derivable from the use of hydraulic fracturing to improve gas and liquid recovery from a gas condensate reservoir operating below dewpoint. This research considers the use of four profit indicators to ascertain the profitability of hydraulic fracturing in a gas condensate reservoir operating below dewpoint by increasing the fracture halflength, fracture width and fracture permeability. The production data of the reservoir was obtained and the economic calculations done on excel spreadsheet and plots generated. The four profit indicators considered in the research are Net Present Value, Payout, Discounted Cash Flow Rate of Return and Profit per Dollar Invested. The economic justification was done by carrying out a comparative economic analysis from the result obtained when the reservoir of study was unfractured with that obtained when the reservoir was fractured at various fracture parameters. The economic analysis was done considering a royalty and tax rate of 18.5% and 30% respectively and a gas price of $2/MSCF and condensate price of $30/bbl. This is done so as to find out if the additional cost of hydraulic fracturing can be offset by the recovery from the reservoir when its pressure declined below dewpoint. The result obtained showed that the additional recovery due to hydraulic fracturing by increasing the fracture halflength, fracture width and fracture permeability was not enough to justify the application of hydraulic fracturing when the reservoir pressure declined below dewpoint.
  • 摘要：The combination of injection of lower saline brine and surfactant will increase recovery in sandstone rocks than either when any of the techniques is singly applied. In this work, core IFT test, pH test, flooding experiments and measurement of dispersion were performed on four core samples which were grouped into two: group A which were not fired and group B which were fired at a temperature of 500°C for 24 hours. Two low saline brines were prepared: LS1 which was derived by the dilution of seawater four times and LS2 which was derived by ten times diluting the seawater. The surfactant used was ethoxylated alcohol surfactant. Coreflood experiments were then performed on the rock samples starting with the injection of low saline followed by low saline brine combined with surfactant (LSS). Results from the experiments show that with the injection of LS1 brine and LSS1 higher increment in recoveries were obtained for group B than for group A cores. The same trend was also noticed with the injection of LS2 and LSS2. From the results, LS1 gave higher increment in oil recovery than LS2. Also LSS1 gave higher recoveries when compared with LSS2. In all the cases tested, core samples which were fired gave higher recoveries even though they had low permeabilities of 993 md for sample 3 and 1017 md for sample 4 than those which were not fired with higher permeabilities of 1050 md and 1055 md for samples 1 and 2 respectively. This was attributed to the alteration of wettability as well as that of permeability caused by sample firing. The dispersion profiles of the rock samples show that all samples are homogeneous.
  • 摘要：Shales have very low permeabilities often within the range of nanodarcies and as such production from shales have been complex and challenging because of poor conductive network. In this work, experiments were conducted to ascertain the effect of matrix acidizing on oil recovery of shale formation in the Niger Delta. Four core samples, S1, S2, S3 and S4 gotten from the Niger Delta shale formation were used. Experiments carried out focused on gas flooding using nitrogen gas at pressures of 1300 psia, 1800 psia and 2300 psia before acid treatment and acidizing with HCL as the choiced acid at different concentrations. XRD was used to analyze the mineral content of the core samples and the analyzed result shows that the predominant mineral constituents of the shale samples are calcite (47%) and dolomite (11%), which are HCl acid soluble constituents. At the end of the experiment, study revealed increase in oil production indicating enhanced productivity as a result of acid treatment and appropriate injection pressure of 800 psia. The result also revealed that the penetration rate in the range of 247.66 min/in to 139.95 min/in before acid treatment decreased to the range 21.67 min/in to 6.61 min/in after acid treatment.
  • 摘要：At present, in the workover operations of old gas wells in the Changqing Gas Field, due to years of exploitation in the production layer, pressure deficits, and general leakage during the well killing, the well must be plugged before the well can be killed. In particular, the fracture-cavity type fractures of the lower paleocarbonate reservoirs have serious leakage. Traditional plugging materials and traditional plugging materials and methods have some limitations in dealing with leakage problems. Therefore, a composite plugging system using polymer solution as the base carrier fluid, multi-particle size rigid particles, expandable particles and modified fibers is developed. Its formula is: water + 2% polyacrylamide + 0.1% N, N-methylene bisacrylamide polymer gel is the base carrier fluid;the formulation of the particle plugging agent was continuously optimized through the CDL-II high temperature and high pressure dynamic and static plugging ability to plug the core. The final formulation of the plugging agent is: 1) 20% rigid particles (5 mm, 1 mm, 0.5 mm CCP-3 ratio 4:2:1) + 1% 3 mm expanded particles SMK-1 + 1% 1 ~ 2 mm fiber SRXW-10;2) 20% rigid particles (3 mm, 0.1 mm, 0.05 mm CCP-3 ratio 3:2:1) + 1% 3 mm expanded particles SMK-1 + 1% 1 ~ 2 mm fiber SRXW-10. The water swelling multiples of the granular plugging agent in salt water are all above 7 times, which meets the requirements of leak-proof plugging operations under high salinity;3% HCl is selected as the gel breaker, and the plugging system has a gel breaking rate of 95%;through the water plugging and profile control experimental system, the sand-filled pipe is used to simulate the plugging effect under high temperature and high pressure, and the plugging system can be sealed for 5 days at a high temperature of 110°C and a high pressure of 20 MPa to achieve a good plugging of the formation. It is expected that the developed plugging system has a good application prospect in future workover operations.
  • 摘要：This project is explaining a laboratory development of a solid free drilling fluid formula that could be potentially used in tight gas reservoirs. The configuration of the weak gel fluid WGL-1, which is resistant to high temperature and high salt, was tested, and concluded that its gelling properties, salt and temperature resistance, and environmental protection were all in line with industry requirements. The final drilling fluid formula was developed as: water + (0.3% ~ 0.5%) NaOH + 5% KCl + 2% WGL-1 + 5% NaCl + (1.0% ~ 2.0%) HBFR Anti-high temperature fluid loss agent + 2% Polyol + (1.5% ~ 2.0%) SDL-1 Lubricant + 0.4% A4O1. The performance of the liquid was tested for temperature resistance, inhibition, gas formation protection effect, plugging performance, and static settlement stability. It was concluded that the temperature resistance performance is satisfied at 150°C, and the cuttings recovery rate is as high as 96.78%. It has good performance in inhibiting water dispersion and swelling of cuttings. The permeability recovery value reaches 88.9%, which meets the requirements of gas formation protection. The SSSI value shows that its settlement stability is good;under high temperature and high pressure, its sealing performance is good. This drilling fluid system has achieved the expected results and laid a foundation for further promoting the development of solid-free drilling fluid systems. The future development direction of solid-free drilling fluids is pointed out, to the improvement of properties to be applied in high temperature environment and have high salt resistance capacity.
  • 摘要：The discharge of pyridine bearing wastewater into water bodies without a prior satisfactory treatment would pose significant public health risk as well as serious threat to the aquatic ecosystems. In this study, a natural shale from Yichang, China is investigated to determine its potential as a low-cost adsorbent for trace pyridine removal from wastewaters. The prepared shale samples without surface modification are characterized by Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD) and scanning electron microscope (SEM). Kinetics and isotherms of pyridine from aqueous solutions onto shale are investigated on the basis of the experimental data. It is found that the shale samples with well-developed porosity are mainly composed of illite, quartz, calcite, chlorite and sericite. Several kinetic models (viz. pseudo-first-order, pseudo-second-order, two-constant rate, intra-particle diffusion and Elovich) as well as isotherm models (Langmuir, Freundlich and Temkin) are applied to test the experimental data for pyridine removal. The kinetics of the adsorption of pyridine by shale follows a pseudo-second-order rate law with the adsorption data being best described by the Freundlich isotherm model. The preliminary study shows that natural shale obtained from sedimentary basins may be used as a potential low-cost adsorbent for the removal of trace pyridine from effluents.
  • 摘要：In this paper, to solve the problems of low water absorption and weak pressure bearing capacity of current plugging materials, acrylic acid (AA), acrylamide (AM), and sodium allyl sulfonate (SAS) are used as monomers, and soluble starch is used as grafting. Material, the use of free radical aqueous solution method to synthesize the plugging agent SWL-1 with good water absorption and strong salt resistance. The monomer ratio is set as n (AA):n (AM):n (SAS) = 5:2:1, the experimental synthesis temperature is 70°C, and the orthogonal experiment is used to determine the experimental synthesis conditions as AA neutralization degree 80%, The amount of initiator is 0.60%, the amount of crosslinking agent is 0.50%, the ratio of monomer to starch is 7:1, and the amount of calcium carbonate is 13%. The comprehensive evaluation of the performance of the plugging agent SWL-1 shows that the water absorption performance at 60°C is the best 268.78 g/g, and the water absorption performance in 8% NaCl, 0.9% CaCl2 and composite brine is 21.5 g/g, 12.5 g/g and 24.9 g/g, indicating good resistance to sodium and calcium, the water retention rate is still higher than 30% after 15 days at 160°C. The sand bed plugging test found that the maximum pressure of SWL-1 was 7 MPa, and the crack plugging test found that when the crack width was 1 mm, 2 mm, and 3 mm, the maximum compressive strength of SWL-1 was 10 MPa. The acid solubility test showed that the maximum pressure was 10 MPa. The highest rate is 86.38%.
  • 摘要：Aiming at the problems of microfracture development in hard brittle shale gas layer in Fuling block, Chongqing, such as collapse of borehole wall and the existence of permeability loss of microfracture during drilling, and serious pollution of drilling environment with oil-based drilling fluid, a water-based drilling fluid system for anti-collapse and anti-leakage was studied. A water-based drilling fluid system with anti-collapse and anti-leakage was formed by introducing functional treatment agents, such as polypolysaccharide MEG, polymer emulsion film forming wall cementing agent LFGB, polyamine inhibitor LCFA and deformable particle plugging agent BXLZ, into the conventional water-based drilling fluid. After rolling at 130°C for 16 h, the system has good rheological properties, low filtration loss, good inhibition, lubrication and plugging properties. It has good plugging properties for 0.12 mm, 0.24 mm, 0.38 mm micro-cracks and 400 mD and 800 mD sand plates. The system was successfully tested on site in August 2019 in Fuling Reef Block, showing good rheological properties, solid wall plugging, and strong ability to seal and inhibit fracture expansion. There was no block falling in the drilling process, and the tripping, casing running and well cementing operations were all smooth, which provided a new technical idea and scheme for environmental protection and green drilling in Fuling shale gas exploitation.
  • 摘要：The phenomenon of petroleum wax deposition is very common during oil well production. When the wax molecule condenses on the surface of the pipeline, it will hinder the exploitation of crude oil, reduce the recovery rate of crude oil, and may lead to the blockage of the pipeline when it is serious, so that the oil recovery work will stop. This phenomenon can be obviously changed by using wax cleaning agent. However, the low ignition point and toxicity of oil-based wax remover are not conducive to oil recovery. Therefore, a new water-based paraffin remover SGJ-1 was developed in this paper. The best formula is: wax dispersant 15%, wetting reversion agent 1%, sodium silicate 1%, alcohol cosolvent 8% and 75% water. Condensation point, wax dissolution rate and anti-wax performance of SGJ-1 water-based dewaxing and anti-waxing agent were tested by self-assembly testing device. The experimental results show that the condensation point of SGJ-1 is -34°C, the viscosity reduction effect is good under 35°C, and the wax dissolution rate is 0.0512 g/min, The highest wax prevention rate can reach 89.58% and the wax removal and wax prevention ability is excellent. Compared with other paraffin removers, SGJ-1 can also reduce the viscosity of crude oil, so it has a good development prospect.
  • 摘要：When drilling deep wells and ultra-deep wells, the downhole high temperature and high pressure environment will affect the emulsion stability of oil-based drilling fluids. Moreover, neither the demulsification voltage method nor the centrifugal method currently used to evaluate the stability of oil-based drilling fluids can reflect the emulsification stability of drilling fluids under high temperature and high pressure on site. Therefore, a high-temperature and high-pressure oil-based drilling fluid emulsion stability evaluation instrument is studied, which is mainly composed of a high-temperature autoclave body, a test electrode, a temperature control system, a pressure control system, and a test system. The stability test results of the instrument show that the instrument can achieve stable testing and the test data has high reliability. This instrument is used to analyze the factors affecting the emulsion stability of oil-based drilling fluids. The experimental results show that under the same conditions, the higher the stirring speed, the better the emulsion stability of the drilling fluid;the longer the stirring time, the better the emulsion stability of the drilling fluid;the greater the oil-water ratio, the better the emulsion stability of the drilling fluid. And the test results of the emulsification stability of oil-based drilling fluids at high temperature and high pressure show that under the same pressure, as the temperature rises, the emulsion stability of oil-based drilling fluids is significantly reduced;at the same temperature, the With the increase in pressure, the emulsion stability of oil-based drilling fluids is in a downward trend, but the decline is not large. Relatively speaking, the influence of temperature on the emulsion stability of oil-based drilling fluids is greater than that of pressure.
  • 摘要：Combined with the current research status in this area at home and abroad, with the improvement of salt and high temperature resistance as the research goal, the laboratory research of salt and high temperature resistant drilling fluid system has been carried out, and lubricants, inhibitors and stabilizers have been optimized. The final drilling fluid formula is: water + 3% sepiolite + 0.3% Na2CO3 + 3% RH-225 + 3% KCOOH + 3% G-SPH + 3% CQA-10 + 1.5% ZX-1 + Xinjiang barite, density 2.2 g/cm3, using hot-rolling furnace, environmental scanning electron microscope, high temperature and high pressure plugging instrument and Zeiss microscopes and other instruments use core immersion experiments, permeability recovery value experiments, and static stratification index methods to perform temperature resistance, reservoir protection, plugging performance, and static settlement stability performance of the configured drilling fluid., Inhibition performance, biological toxicity, salt resistance, anti-pollution performance have been tested, and it is concluded that the temperature resistance is good under the condition of 210°C, and the salt resistance can meet the requirements of 20% NaCl + 0.5% CaCl2 concentration. It has a good reservoir protection effect, the permeability recovery value can reach more than 90%, the performance of restraining water dispersion and cuttings expansion is good, the heat roll recovery rate can reach more than 85%, and the SSSI value shows that its settlement stability performance is good;Its plugging performance is good under high temperature and high pressure. It laid the foundation for the next step to promote the field application of the drilling fluid system.
  • 摘要：Based on the difference of wave impedance between sand layer and surrounding rock, the seismic wave numerical simulation software, Tesseral-2D is used to establish the sandstone formation model containing water, oil and gas respectively, and the three models are treated by post-stack time offset under the conditions of defined channel spacing, wavelet frequency and wave velocity of different rock mass, and the root means square amplitude difference attribute profile under the condition of water-filled oil-filled and gas-filled oil-filled is obtained. From this, it can be obtained that after oil-gas substitution occurs in weak non-mean reservoirs, the root-mean-square amplitude difference from the reservoir to the lower part of the reservoir experiences a mutation process from a positive maximum to a negative maximum, while after oil-water substitution, the root-mean-square amplitude difference from the reservoir to the lower part of the reservoir experiences a mutation process from zero to a positive maximum. For a strong heterogeneous reservoir. Therefore, for Weak inhomogeneous media similar to tight sandstone, the root-mean-square amplitude difference attribute can be used to detect the distribution of fluid in the actual gas drive or water drive oil recovery process.
  • 摘要：In view of the fact that most of the filter media of existing plugging evaluation instruments use steel plates or steel balls, which cannot truly simulate the characteristics of the formation, a new type of TL-1 high temperature and high pressure plugging instrument has been developed. The filter medium of the instrument is the natural stone with different cracks and quartz sand beds with different particle sizes, which can better simulate the adsorption and hang-up effect of the formation on the plugging agent. It is possible to evaluate the plugging effect, pressure-bearing capacity and return pressure of the plugging slurry for different cracks and sand beds of different sizes under different temperatures and pressures. Using new and old instruments to evaluate the plugging effect of the same plugging slurry, it is found that the plugging effect is different from the distribution of the plugging material on the crack surface, the plugging effect and the pressure bearing capacity. The instrument is stable and reliable in operation and simple in operation. It is a new instrument for conducting research on anti-leakage plugging materials and anti-leakage plugging drilling fluid systems.
  • 摘要：Traditional methods for judging the degree of insufficient fluid supply in oil wells have low efficiency and limited accuracy. To address this problem, a method for intelligently identifying the degree of insufficient fluid supply in oil wells based on convolutional neural networks is proposed in this paper. Firstly, 5000 indicator diagrams with insufficient liquid supply were collected from the oilfield site, and a sample set was established after preprocessing;then based on the AlexNet model, combined with the characteristics of the indicator diagram, a convolutional neural network model including 4 layers of convolutional layers, 3 layers of down-pooling layers and 2 layers of fully connected layers is established. The backpropagation, ReLu activation function and dropout regularization method are used to complete the training of the convolutional neural network;finally, the performance of the convolutional neural network under different iteration times and network structure is compared, and the super parameter optimization of the model is completed. It has laid a good foundation for realizing the self-adaptive and intelligent matching of oil well production parameters and formation fluid supply conditions. It has certain application prospects. The results show that the accuracy of training and verification of the method exceeds 98%, which can meet the actual application requirements on site.
  • 摘要：Accurate determination of hydraulic parameters such as pressure losses, equivalent circulation density (ECD), etc. plays profound roles in drilling, cementing and other well operations. Hydraulics characterization requires that all factors are considered as the neglect of any could become potential sources of errors that would be detrimental to the overall well operation. Drilling Hydraulics has been extensively treated in the literature. However, these works almost entirely rely on the assumption that the drill string lies perfectly at the center of the annulus—the so-called “concentric annulus”. In reality, concentricity is almost never achieved even when centralizers are used. This is because of high well inclination angles and different string geometries. Thus, eccentricity exists in practical oil and gas wells especially horizontal and extended reach wells (ERWs) and must be accounted for. The prevalence of drillstring (DS) eccentricity in the annulus calls for a re-evaluation of existing hydraulic models. This study evaluates the effect of drilling fluid rheology types and DS eccentricity on the entire drilling hydraulics. Three non-Newtonian fluid models were analyzed, viz: Herschel Bulkley, power law and Bingham plastic models. From the results, it was observed that while power law and Bingham plastic models gave the upper and lower hydraulic values, Herschel Bulkley fluid model gave annular pressure loss (APL) and ECD values that fall between the upper and lower values and provide a better fit to the hydraulic data than power law and Bingham plastic fluids. Furthermore, analysis of annular eccentricity reveals that APLs and ECD decrease with an increase in DS eccentricity. Pressure loss reduction of more than 50% was predicted for the fully eccentric case for Herschel Bulkley fluids. Thus, DS eccentricity must be fully considered during well planning and hydraulics designs.
  • 摘要：The South Malang Region is located in the south-eastern part of the Southern Mountain Volcanic Arc;it presents different opportunities for hydrocarbon exploration. The stratigraphy of the study area from old to young consists of Oligocene Volcanic rocks (Mandalika, Watupatok, and Arjosari Formation), Early Miocene Carbonates (Campurdarat and Jaten Formation), Middle Miocene Volcanic (Wuni Formation), Late Miocene-Pliocene Carbonates (Nampol, Oyo, and Wonosari Formation), and Holocene alluvial deposits (Kalipucang Formation). The dominance of volcanic rocks makes this area considered an area without hydrocarbon play prospects. Petroleum system potential is revealed by evaluating and analyzing potential source rock and reservoir rock outcrop samples. The study shows that the Nampol Formation can be considered as a gas-prone source rock, with type III kerogen, total organic content ranging from 3.48 - 26.18 wt%, and possess the potential to produce good to very good hydrocarbons and a hydrogen index ranging from 43 to 86 mgHC/g TOC. Furthermore, rock core analysis and petrographic studies were carried out on the Nampol sandstone where the rock samples showed good reservoir properties. However, the Nampol and Wonosari limestone that was considered as the secondary target for reservoir possesses a low quality of reservoir properties. This study shows that there is a potential for petroleum system existence in the Southern Mountain subvolcanic arc, which is indicated by the presence of source rock and potential reservoir rock as one of the various elements and processes present in a petroleum system.
  • 摘要：Seeking effective solutions to control and mitigate the interaction between drilling fluids and clay formations has been a challenge for many years, and various shale inhibitors have shown excellent results in problematic shale formations around the world. Herein, the hyperbranched polyamine (HBPA) inhibitor with a higher ratio of amine groups and obvious tendentiousness in protonation was successfully synthesized from ethylenediamine, acryloyl chloride and aziridine by five steps, in which the metal-organic framework (MOF) was employed as a catalyst for ring-open polycondensation (ROP). The structure and purity were confirmed by nuclear magnetic resonance hydrogen spectroscopy and high-performance liquid chromatography (HPLC) respectively. The HBPA displays more excellent performance than EDA and KCl widely applied in the oil field. After aging at 80°C and 180°C, the YP of a slurry system containing 25 wt.% bentonite and 2 wt.% HBPA are just 8.5 Pa and 5.5 Pa (wt.%: percentage of mass), respectively. The swelling lengths of 2 wt.% HBPA are estimated to be 1.78 mm, which falls by 70% compared with that of freshwater. Under a hot rolling aging temperature of 180°C, the HBPA system demonstrates a significant inhibition with more than 85% shale cuttings recovery rate and is superior to conventional EDA and KCl. Mechanism analysis further validates that the HBPA can help to increase the zeta potential.
  • 摘要：To supplement, adjust and improve the division plan of crude oil strata in the west of Mahuangshan Mountain. Combining well logging, core, and drilling analysis and testing data, Petrel software was utilized to classify and compare the 10 layers of the Yan’an Formation. Draw 6 “net-like” skeleton profiles for Ningdong No. 2 and No. 3 wells, involving 31 wells. On the basis of the large-layer strata division, Yan 8 and Yan 9 sections are divided and compared;five “net-like” skeleton profiles were drawn in the 5 well, involving 16 wells. On the basis of the large-layer division, the small-layer division and comparison were performed by Yan 8 and Yan 9. The results show that the Yan 8 oil layer is divided into two stratigraphic units, and Yan 8 and Yan 82, and the Yan 9 oil layer is divided into two stratigraphic units, Yan 91 and Yan 92;the Yan 2 layer in the 2 and 3 well blocks of Ningdong is in the marker layer. The top of the coal seam, Yan 8 layers in the Ningdong 5 well area is on the top of the auxiliary marker seam. The fine division of small layers into tiny layers of sedimentary microfacies, reservoir heterogeneity, development dynamic analysis, remaining oil distribution and other studies provide indispensable data.
  • 摘要：With the innovation and development of offshore oil drilling technology, drilling wells in deep waters areas have become an important activity for the development of new hydrocarbon reservoirs in this type of environment. CNOOC (China National Offshore Oil Corporation) won the rights to exploit two unexplored deepwater blocks in the Gulf of Mexico, in a bid realized by the Mexican Government (CNH), in 2016. The challenge to combine the newest technology with the oil industry experienced knowledge to lead the exploration and development of these deep-water blocks in Mexico is around the corner. Therefore, the basic techniques for deep waters wells drilling and the main potential risks are expounded in this paper. A set of deep waters wells drilling processes and methodologies are previously designed, and a specific case is demonstrated next, which provides a referential model for deep waters wells drilling in the Gulf of Mexico.

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