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Development and characterization of an automated nanofiltration apparatus.

机译:自动化纳滤设备的开发和表征。

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Conventionally membrane research implements cross-flow filtration scheme to reduce membrane fouling. The control and optimization of such membrane apparatus have been tedious due to the simultaneous change of various parameters such as applied pressure, flow rate of feed, permeate and concentrate, and feedwater recovery during the course of membrane filtration. Since the accurate control of the operating parameters is critical for data quality, it becomes imperative to have system being controlled automatically. Automatic data acquisition and control ensures accurate data collection and that the data generated are more reliable and with minimum possible errors.; In this study, a fully automated cross flow nanofiltration apparatus has been successfully developed and characterized. Using LabVIEW as a programming language, it has been possible to completely automate the filtration system. System is designed to control two parameters and acquire two additional data simultaneously. Numbers of experiments have been carried out to optimize control parameters such as acquisition rate, number of samples per second, various control parameters for two controllers etc.; A detailed and user-friendly front panel (user interface) has been developed to make system easy to use. This panel shows two plots showing trend of all the parameters. It also has auto-manual selection switch, knob for valve opening selection in manual mode, set point selectors and indictors for all present value. It does give smooth mode transfer from manual to auto.; It is observed that best rate for the data acquisition is 100 samples/sec with 100 samples averaged every second. The optimum control parameters, obtained by Ziegler-Nickols technique, for flow controller are: Kc = 0.26, Ti = 0.0335 mins, Td = 0.00837 mins. These parameter for the pressure controller are found to be: Kc = 0.0195, Ti = 0.05 mins, Td = 0.0125 mins.
机译:常规地,膜研究实施错流过滤方案以减少膜结垢。由于在膜过滤过程中同时改变了各种参数,例如施加压力,进料,渗透液和浓缩液的流速以及进料水的回收率,这种膜装置的控制和优化非常繁琐。由于对操作参数的精确控制对于数据质量至关重要,因此必须对系统进行自动控制。自动数据采集和控制可确保精确的数据收集,并确保生成的数据更可靠且错误最少。在这项研究中,已经成功开发并表征了一种全自动的错流纳滤装置。使用LabVIEW作为编程语言,可以使过滤系统完全自动化。系统旨在控制两个参数并同时获取两个附加数据。已经进行了许多实验以优化控制参数,例如采集速率,每秒样本数,两个控制器的各种控制参数等;开发了详细且用户友好的前面板(用户界面),以使系统易于使用。此面板显示两个曲线图,显示所有参数的趋势。它还具有自动手动选择开关,用于在手动模式下选择阀门开度的旋钮,用于所有当前值的设定点选择器和指示器。确实可以实现从手动到自动的平稳模式转换。可以看出,数据采集的最佳速率是100个样本/秒,每秒平均100个样本。通过Ziegler-Nickols技术获得的流量控制器的最佳控制参数为:Kc = 0.26,Ti = 0.0335分钟,Td = 0.00837分钟。发现压力控制器的这些参数为:Kc = 0.0195,Ti = 0.05分钟,Td = 0.0125分钟。

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