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In situ crystal growth imaging during explosive crystallization

机译:爆炸结晶过程中的原位晶体生长成像

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摘要

Explosive crystallization of amorphous germanium of 0.89 and 1.80 microns in thickness deposited on quartz substrates was investigated. A scalloped, mixed, and columnar regime was observed. In situ images captured using dark field imaging reveal the shape of the explosive crystallization front. Crystallization was induced by a frequency tripled Nd:YAG laser (λ = 355 nm) focused to a tight line. A second Nd:YAG laser was frequency doubled (λ = 532 nm) and used as an illumination source for two time resolved pictures. The shape and speed of the explosive crystallization front is observed for various heat loss parameters and crystallization regimes and is generally in good agreement with the literature. Surface morphology is inspected by Atomic Force Microscopy (AFM) after explosive crystallization has completed.
机译:研究了沉积在石英衬底上的厚度为0.89和1.80微米的非晶锗的爆炸结晶。观察到扇贝形,混合形和柱状形。使用暗场成像捕获的原位图像揭示了爆炸物结晶前沿的形状。通过倍频Nd:YAG激光(λ= 355 nm)聚焦到一条紧线来诱导结晶。将第二个Nd:YAG激光器的频率加倍(λ= 532 nm),并用作两个时间分辨图片的照明源。对于各种热损失参数和结晶方式,可观察到爆炸结晶前沿的形状和速度,并且通常与文献一致。爆炸结晶完成后,通过原子力显微镜(AFM)检查表面形态。

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