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A green approach to preparing nanosized hollow silica microspheres with waste polystyrene

机译:用废聚苯乙烯制备纳米级空心二氧化硅微球的绿色方法

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An attempt was made to prepare hollow silica microspheres by an oil-in-water emulsion which proposed to use waste polystyrene organic solution as oil phase. Effects of the kinds and amounts of surfactants and the concentration of waste polystyrene solution on the nanosized hollow silica microspheres were studied. The prepared hollow silica microspheres were characterized by TEM, XRD, TG-DTA and particle size distribution analyzer. The experimental results showed that the waste polystyrene organic solution was successfully treated as oil core and the cores could be removed at about 350℃. Meanwhile, the obtained hollow microspheres were amorphous with an average particle size of 40nm. The hollow silica microspheres could be obtained with the selected surfactant.
机译:尝试通过水包油乳液制备空心二氧化硅微球,该乳液建议使用废弃的聚苯乙烯有机溶液作为油相。研究了表面活性剂的种类和数量以及废聚苯乙烯溶液的浓度对纳米级中空二氧化硅微球的影响。通过TEM,XRD,TG-DTA和粒度分布分析仪对制备的空心二氧化硅微球进行了表征。实验结果表明,该废聚苯乙烯有机溶液已成功地作为油核,在约350℃时可以去除核。同时,获得的中空微球是无定形的,平均粒径为40nm。用所选择的表面活性剂可以获得中空的二氧化硅微球。

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