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Coconut husk ash as heterogenous catalyst for biodiesel production from cerbera manghas seed oil

机译:椰子壳灰作为Cerbera Manghas Seed油的生物柴油生产的异质催化剂

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The research on the use of coconut husk as a solid catalyst for transesterification reaction of Cerbera manghas oil into biodiesel has been done. The aim of this study is to investigate the performance of coconut husk ash for biodiesel production from Cerbera manghas seed oil. Coconut husk is prepared by burning in air to obtain potassium oxide as active phase. The coconut husk is analyzed by X-ray diffraction (XRD) and scanning electron microscopy (SEM). The XRD spectrum shows that the peak characteristics of potassium oxide can be observed in the diffractogram. The particle size of the catalyst ranging from 1 - 3 μm with pentagonal structure. The coconut husk ash solid catalyst is used in the transesterification reaction of Cerbera manghas oil in a batch reactor. Biodiesel yield of 88.6% can be achieved over coconut husk ash catalyst, using a 10 wt.% of catalyst, reaction temperature at 3 hours, and a methanol-to-oil ratio of 6: 1. This solid catalyst can be separated easily from the reaction system and not soluble in methanol or methyl esters. The coconut husk ash catalyst is high potential to be developed as one of the solid catalysts to convert Cerbera manghas oil to biodiesel.
机译:已经完成了用椰子壳作为Cerbera Manghas Into在生物柴油中的酯交换反应的固体催化剂的使用研究。本研究的目的是探讨椰子壳灰对Cerbera Manghas Seed油的生物柴油生产的表现。通过在空气中燃烧以获得氧化钾作为活性相的椰子壳。通过X射线衍射(XRD)和扫描电子显微镜(SEM)分析椰子壳。 XRD光谱表明氧化钾的峰特性可以在衍射图中观察到。催化剂的粒径为1-3μm,具有五角形结构。椰子壳灰分固体催化剂用于批量反应器中Cerbera Manghas油的酯交换反应。通过椰子壳灰催化剂,使用10重量%的催化剂,3小时的反应温度和6:1的甲醇与油比的生物柴油蛋白酶产率可以实现88.6%。该固体催化剂可以容易地分离反应体系,不溶于甲醇或甲酯。椰子壳灰催化剂具有高潜力,以开发为将Cerbera Manghas Oil到生物柴油转化的固体催化剂之一。

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