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Effects of deposition temperature on the synthesis of single and multi wall carbon nanotubes from palm oil by floated catalyst TCVD method

机译:沉积温度对絮状催化剂TCVD法从棕榈油合成单壁碳纳米管的影响

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This paper will report on the synthesization of single wall carbon nanotubes (SWCNTs) and multiwall carbon nanotubes (MWCNTs) from palm oil precursor and ferrocene as catalyst source by single zone thermal CVD system at various deposition temperature ranging from 600–1000°C. Direct heat was used to vaporize both fixed parameter of precursor and catalyst placed in the middle of quartz tube. Field emission scanning electron microscopy was used to obtain the image of CNTs which showed different structures and diameters of CNTs relative to the deposition temperature of furnace. Raman Spectroscopy and energy dispersive X-ray were then used to further study the crystallinity, weight percentage and identification of samples.
机译:本文将通过单区域热CVD系统在各种沉积温度范围为600-1000&#x00b0,从棕榈油前体和二茂铁作为催化剂源的单壁碳纳米管(swcnts)和多壁碳纳米管(mwcnts)的合成。 。 直接热用于蒸发置于石英管中间的前体和催化剂的固定参数。 场发射扫描电子显微镜用于获得相对于炉子沉积温度显示CNT的CNT的图像,其显示为CNT的不同结构和直径。 然后使用拉曼光谱和能量分散X射线进一步研究结晶度,重量百分比和样品的鉴定。

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