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Electrochemical Study of Graphene-NiCo_2O_4 Nanocomposite Prepared Through Solvothermal Approach

机译:通过溶剂热方法制备石墨烯-NICO_2O_4纳米复合材料的电化学研究

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A green approach was employed for the synthesis Graphene-NiCo2O_4 nanocomposite and its electrochemical property has been studied. The formation of phase and morphology was studied by diffraction and microscopic analysis. The prepared material was studied as an electrode material for supercapacitor application in a 2 M KOH electrolyte. In order to examine the electrochemical behavior of the prepared material cyclic voltammetry (CV), Galvanostatic charge-discharge (GCD) and electrochemical impedance spectroscopy (EIS) measurements were carried out in a 3-electrode system. Electrochemical studies revealed a high specific capacitance of 242 F g~(-1) and 165 F g~(-1) were obtained at a high scan rate of 10 mV s~(-1) and at an applied current density of 0.5 A g~(-1), respectively. A high initial capacitance retention value and coulombic efficiency of about 96% and 98% was retained after a long 1000 discharge cycles. Hence, the prepared material can be a potential candidate for high performance supercapacitor applications.
机译:用于合成石墨烯-NICO2O_4纳米复合材料的一种绿色方法,研究了其电化学性能。通过衍射和微观分析研究了相和形态的形成。将制备的材料作为超级电容器施加的电极材料,以2M KOH电解质应用。为了检查制备的材料循环伏安法(CV)的电化学行为,在3电极系统中进行电化电荷 - 放电(GCD)和电化学阻抗光谱(EIS)测量。电化学研究揭示了242f g〜(-1)和165f g〜(-1)的高比电容,以10 mv s〜(-1)的高扫描速率,施加电流密度为0.5 a g〜(-1)分别。在长1000个放电循环之后,保留高初始电容保持值和约96%和98%的库仑效率。因此,制备的材料可以是高性能超级电容器应用的潜在候选者。

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