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Synthesis and Crystal structure of 1-(3,5-dichloro-2-hydroxyphenyl)-3-(5-methylfuran-2-yl)prop-2-en-1-one

机译:1-(3,5-二氯-2-羟基苯基)-3-(5-甲基呋喃-2-基)PROP-2-EN-1-1的合成和晶体结构

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摘要

The title compound, Cl_(4)Hl_(0)Cl_(2)O_(3), was synthesized and recrystallized from an organic solution and crystallizes in monoclinic system with space group P 21/c. The crystal structure analysis and the molecular arrangement of these crystals are determined using X-ray diffraction method. The molecule is almost planar as evidenced by the very low values of torsion angles. The hydroxy group substituted at C16 position is in anti-periplanar conformation with respect to the phenyl ring.
机译:标题化合物,Cl_(4)HL_(0)Cl_(2)O_(3)被合成并从有机溶液中重结晶,并在具有空间组P 21 / C的单斜液系统中结晶。使用X射线衍射法测定这些晶体的晶体结构分析和分子布置。分子几乎是平面,如扭转角度的非常低的值证明。取代在C16位置的羟基是相对于苯环的抗预升性构象。

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