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Preparation and Characterization of Fe-ACF/TiO2 Composites and their Photocatalytic Activity

机译:Fe-ACF / TiO2复合材料的制备,表征及其光催化活性

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In this study,we have prepared Fe-ACF(activated carbon fiber)/TiO2 composites with titanium(VI)n-butoxide(TNB1 as titanium source to activated carbon fiber pre-treated with jron compound through the impregnation method,As a basic property for the composites,the results of the textural surface properties demonstrate that there is a slight decrease n the BET surface area of composite samples with an increase of the amount of iron compound treated.The surface morphology for the Fe-ACF/TiO2,composites was characterized by SEM,which presents to the porous texture on the composites and the homogenous compositions for Fe and titanium dioxide distributed on the sample surfaces.The phase formation and stmctural transition for the iron compound and titanium dioxide were observed in the X-ray diffraction patterns for the Fe-ACF/TiO2 composites.The cherfiical composition for the Fe-ACF/TiO2 composites was investigated with EDX,which showed stronr peaks for C,O,Fe and Ti element.From the photo degradation results,the Fe-ACF/TiO2 composites showed the excellent removal activity for the COD due to photocatalysis of the supported TiO2,radical reaction by Fe species and adsorptivity and absorptivity of ACF.
机译:本研究以浸渍法制备了以铁(jron)化合物预处理的活性炭纤维,以正丁醇钛(VIB)(TNB1)为钛源,制备了Fe-ACF(活性炭纤维)/ TiO2复合材料。对于复合材料,结构表面性能的结果表明,随着铁化合物​​处理量的增加,复合材料样品的BET表面积略有减少。Fe-ACF/ TiO2复合材料的表面形态为用SEM表征,在复合材料上呈现出多孔结构,并在样品表面分布了均匀的Fe和二氧化钛成分.X射线衍射图中观察到铁化合物和二氧化钛的相形成和结构转变用EDX对Fe-ACF / TiO2复合材料的化学成分进行了EDX分析,结果显示了C,O,Fe和Ti元素的锶峰。结果表明,Fe-ACF / TiO2复合材料由于负载型TiO2的光催化作用,Fe的自由基反应以及ACF的吸附性和吸收性,对COD的去除效果极好。

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