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A low-temperature synthesis of ZnO/ carbon nanotubes nanocomposites

机译:ZnO /碳纳米管纳米复合材料的低温合成

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The self-assembled heterojunctions of ZnO nanoparticles and multi-wall carbon nanotubes (MWNT) were prepared by employing Zn(CH3COO)2·2H2O, NaOH as the starting materials in the presence of polyethylene glycol (PEG). The MWNT was functionalized via the sol-gel method at ambient pressure and low temperature. The resultant materials were characterized by X-ray powder diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and Fourier transfer infrared spectra (FTIR) measurement. The results revealed intimate contact between the ZnO nanoparticles and MWNT, and that PEG played a significant role in the formation of the ZnO/MWNT nanocomposites. Under mild reaction conditions, ZnO crystallites have a very uniform size distribution and average cross-sectional dimensions of 80-150 nm.
机译:在聚乙二醇(PEG)存在下,以Zn(CH3COO)2·2H2O,NaOH为起始原料,制备了ZnO纳米颗粒和多壁碳纳米管(MWNT)的自组装异质结。通过溶胶-凝胶法在环境压力和低温下将MWNT官能化。通过X射线粉末衍射(XRD),扫描电子显微镜(SEM),透射电子显微镜(TEM)和傅立叶转移红外光谱(FTIR)测量来表征所得材料。结果表明,ZnO纳米颗粒与MWNT之间紧密接触,而PEG在ZnO / MWNT纳米复合材料的形成中起着重要作用。在温和的反应条件下,ZnO微晶具有非常均匀的尺寸分布和80-150 nm的平均横截面尺寸。

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