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Generation of Nickel Oxide Nanoparticles by Wire Explosion Process and Its Interaction with Glucose

机译:线爆炸法制备氧化镍纳米粒子及其与葡萄糖的相互作用

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Nickel oxide (NiO) nanoparticles were produced by wire explosion process (WEP) in Oxygen ambience. XRD studies have confirmed the formation of NiO during WEP under oxygen rich environment and with high energy ratios. Crystallite size of synthesized NiO nanoparticles was found to be 26.7 nm. The particles produced are spherical in shape as evident from the microstructural characterizations. Ultraviolet-visible (UV-vis) spectroscopy analysis was made to obtain the band gap of NiO nanoparticles. Thermodynamics aspect of NiO nanoparticles formation were detailed using classical homogeneous nucleation theory. The potential application of NiO as Bio sensor for Glucose sensing was demonstrated using UV-vis spectroscopy, with a detection limit of 42μM.
机译:氧化镍(NiO)纳米粒子是在氧气环境中通过线爆炸法(WEP)制成的。 XRD研究证实了在富氧环境下高能量比的WEP期间NiO的形成。发现合成的NiO纳米颗粒的微晶尺寸为26.7nm。从微观结构表征可以明显看出,所产生的颗粒为球形。进行紫外-可见(UV-vis)光谱分析以获得NiO纳米颗粒的带隙。使用经典的均相成核理论详细描述了NiO纳米颗粒形成的热力学方面。使用紫外-可见光谱法证明了NiO作为生物传感器进行葡萄糖感测的潜在应用,其检测极限为42μM。

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