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Preparation Of Graphene Oxide/Conducting Polymer Nanocomposites By Rf-Plasma Polymerization

机译:Rf-等离子聚合制备氧化石墨烯/导电聚合物纳米复合材料

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have some advantages include: environmental friendliness of the solvent-free preparation; conducting polymers can be directly coated on material surfaces; the obtained materials can be used directly without purification; the thickness of the film can be controlled by changing the treatment time; fast and cost effective. In this work, three different nanocomposites of graphene oxide and conducting polymer (polythiopene, polyaniline and polypyrrole) were prepared through RF-rotating plasma method. The reaction conditions as follows: 13.56 MHz, pressure of 0.02 Torr, power of 40W and reaction time of 3h. The nanocomposites were investigated in terms of morphology, structure, adn thermal behaviors with scanning electron microscopy (SEM), Fourier-transform infrared spectroscopy (FT-IR), X-ray photoelectron spectroscopy (XPS) and thermal gravimetric analysis (TGA).
机译:具有的一些优点包括:环保的无溶剂制备方法;导电聚合物可以直接涂覆在材料表面上;所得材料无需纯化即可直接使用;膜的厚度可以通过改变处理时间来控制。快速且具有成本效益。在这项工作中,通过射频旋转等离子体方法制备了三种不同的氧化石墨烯和导电聚合物纳米复合材料(聚噻吩,聚苯胺和聚吡咯)。反应条件如下:13.56MHz,压力为0.02Torr,功率为40W,反应时间为3h。使用扫描电子显微镜(SEM),傅立叶变换红外光谱(FT-IR),X射线光电子能谱(XPS)和热重分析(TGA)对纳米复合材料的形貌,结构,热行为进行了研究。

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