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Field Applications of Ion Mobility Spectrometry

机译:离子迁移谱的现场应用

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摘要

Ion mobility spectrometry (IMS) is an excellent tool for detection of controlled substances under field conditions. Plasmagrams and tables showing the results of field applications will be discussed. Residues of drugs, such as cocaine and heroin, can be left anywhere including vehicles, boats, and houses. In houses, the carpets, walls, and floors are good locations for residues to adhere. Individual clothing can also be contaminated with drug residue. Vehicles that are suspected of having previously smuggled illegal substances can b e vacuumed and screened. Tablets that look similar and respond the same when screened with the Marquis reagent can be differentiated by IMS. With Southern California being the "methamphetamine capital of the world" and the resurgence of phencyclindine (PCP), IMS has proven extremely valuable in the screening of abandoned clandestigne alboratory sites and vehicles in which the clandestine laboratories' chemicals and glassware were transported. IMS is very responsive to ephedrine/pseudoephedrine, a precursor of methamphetamine and 1-piperidinocyclohexanecarbonitrile (PCC), an intermediate of phencylindine. Once residues are detected, vacuumsamples, and/or metanol wipes are collected and analyzed at the DEA Laboratory for confirmaton of the suspected substance using GC-IRD or Mass Spectrometry.
机译:离子迁移谱(IMS)是在野外条件下检测受控物质的出色工具。将讨论显示现场应用结果的血浆图和表格。可卡因和海洛因等毒品的残留物可以留在任何地方,包括车辆,船只和房屋。在房屋中,地毯,墙壁和地板是残留物附着的好位置。单独的衣服也可能被药物残留污染。怀疑以前曾走私违禁物质的车辆可以进行吸尘和检查。 IMS可以区分使用Marquis试剂进行筛选时外观相似且反应相同的平板电脑。由于南加州是“世界甲基苯丙胺之都”,苯环己定(PCP)的兴起,IMS已被证明在筛选废弃的秘密实验室地点和运输秘密实验室化学药品和玻璃器皿的车辆中具有极其重要的价值。 IMS对麻黄碱/伪麻黄碱(一种甲基苯丙胺和1-哌啶子基环己烷甲腈(PCC)的一种前体)的反应非常敏感。一旦检测到残留物,就将收集真空样品和/或甲醇擦拭布,并在DEA实验室进行分析,以使用GC-IRD或质谱法确认可疑物质。

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