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Tailoring the mechanical properties of SU-8/clay nanocomposites: polymer microcantilever fabrication perspective

机译:量身定制SU-8 /粘土纳米复合材料的机械性能:聚合物微悬臂梁的制造前景

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SU-8/Clay nanocomposite is considered as a candidate material for microcantilever sensor fabrication. Organically modified montmorillonite clay nanoparticles are dispersed in the universally used negative photoresist polymer SU-8, for a low cost material, which is also biocompatible. If varying the clay loading of the composite material yields a variation of the Young's modulus, the tailored material stiffness presents an opportunity for fabrication of microcantilevers with tunable sensor sensitivity. With this microcantilever application perspective, mechanical and thermal properties of the material were investigated. SU-8/Clay nanocomposite samples were prepared with clay loadings from lwt% - 10wt%. Tensile test results show a general trend of increase in composite modulus with an increase in the clay loading up to 7wt%, followed by a small drop at 10wt%. The composite material indeed yields moderate variation of the Young's modulus. It was also found that the thermal degradation peak of the material occurred at 300°C, which is beyond the operating temperature of typical microcantilever sensor applications. The fabrication of a custom designed microcantilever array chip with the SU-8/Clay nanocomposite material was achieved in a class 100 cleanroom, using spin-coating and photolithography microfabrication techniques. The optimization of the process for fabricating microcantilever with the SU-8/Clay nanocomposite material is discussed in this paper. The results of this research are promising for cheaper mass production of low cost disposable, yet sensitive, microcantilever sensor elements, including biosensor applications.
机译:SU-8 /粘土纳米复合材料被认为是微悬臂梁传感器制造的候选材料。将有机改性的蒙脱土粘土纳米颗粒分散在通用的负性光刻胶聚合物SU-8中,这是一种低成本的材料,也是生物相容的。如果改变复合材料的粘土载荷会产生杨氏模量的变化,则定制的材料刚度将为制造具有可调传感器灵敏度的微悬臂梁提供机会。从这种微悬臂梁应用的角度出发,研究了材料的机械性能和热性能。制备的SU-8 /粘土纳米复合材料样品的粘土负载量为1wt%-10wt%。拉伸试验结果表明,复合模量增加的总体趋势是粘土加载量增加到7wt%,然后在10wt%时有小幅下降。实际上,复合材料会产生适度的杨氏模量变化。还发现该材料的热降解峰出现在300°C,超过了典型的微悬臂梁传感器应用的工作温度。使用旋涂和光刻微细加工技术,在100级无尘室中完成了采用SU-8 /粘土纳米复合材料定制设计的微悬臂阵列芯片的制造。本文讨论了SU-8 /粘土纳米复合材料制备微悬臂梁工艺的优化。这项研究的结果有望以低成本批量生产低成本的一次性,但灵敏的微悬臂梁传感器元件,包括生物传感器应用。

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