Synthesizing hexanitrohexaazaisowurtzitane, comprises performing hexa-N-deallylation of 2,4,6,8,10,12-hexaallyl-2,4,6,8,10,12-hexaazatetracyclo(5.5.0.0(5.9).0(3.11))dodecane or hexaallylisowurtzitane, in an organic solvent, in the presence of a reducing agent, a catalyst and a deallylated amino function protecting agent in a stoichiometric molar ratio, where the protecting agent protects 2-4 deallylated amino functions in 2, 6, 8 and 12 positions substituted by nitro group for nitration of protected amino functions, and performing nitration of the protected amino functions. An independent claim is included for synthesis intermediate consisting of 2,6,8,12-tetra(1-6C-alkyl, 1-6C-alkylene or benzyl)carbamate hexaazaisowurtzitane, 2,6,8-tri(1-6C-alkyl, 1-6C-alkylene or benzyl)carbamate hexaazaisowurtzitane and 2,8-di(1-6C-alkyl, 1-6C-alkylene or benzyl)carbamate hexaazaisowurtzitane, preferably 2,6,8,12-tetra-di-tert-butyl dicarbonate-hexaazaisowurtzitane, 2,6,8-tri-di-tert-butyl dicarbonate-hexaazaisowurtzitane, 2,8-di-di-tert-butyl dicarbonate-hexaazaisowurtzitane, 2,6,8,12-tetra-methoxycarbonyl-hexahexaazaisowurzitane, 2,6,8-tri-methoxycarbonyl-hexaazaisowurtzitane, 2,8-di-methoxycarbonyl-hexaazaisowurtzitane, 2,6,8,12-tetra-ethyloxycarbonyl-hexaazaisowurtzitane, 2,6,8-tri-ethyloxycarbonyl-hexaazaisowurtzitane, or 2,8-di-ethyloxycarbonyl-hexaazaisowurtzitane.
展开▼
