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Advanced heavy metal pollution source identification method in contaminated soils and stream sediments using isotope analysis of heavy minerals

机译:重矿物同位素分析的先进土壤重金属污染源识别方法

摘要

According to the present invention, a method for analyzing a heavy metal contamination source of contaminated soil and river deposit by isotope analysis of heavy minerals comprises the steps of: (a) separating heavy minerals from a sample including heavy metals; (b) putting the heavy minerals of step (a) into a Teflon vial, adding an acidic solution, heating the same, dissolving the same, and drying the same; (c) putting hydrochloric acid into the dried heavy minerals of step (b), heating the same, drying the same, and dissolving the same in hydrogen bromide; (d) centrifuging the heavy minerals dissolved in hydrogen bromide in step (c), and separating heavy metals using an anion exchange resin and hydrogen bromide; and (e) analyzing heavy metals separated in step (d). According to the present invention, the method for analyzing a heavy metal contamination source of contaminated soil and river deposit by isotope analysis of heavy minerals has an advantage of more accurately analyzing the artificial origin and the natural origin of a contamination source of heavy metals, specifically Pb, by separating and obtaining heavy minerals in contaminated soil and river deposit and by performing isotope analysis.
机译:根据本发明,一种通过同位素分析重矿物来分析土壤和河流沉积物的重金属污染源的方法,包括以下步骤:(a)从包括重金属的样品中分离重矿物; (b)将步骤(a)的重矿物放入聚四氟乙烯瓶中,加入酸性溶液,加热,溶解,干燥。 (c)将盐酸放入步骤(b)的干燥重矿物中,加热,干燥,将其溶解在溴化氢中; (d)将步骤(c)中溶解于溴化氢中的重矿物离心分离,并使用阴离子交换树脂和溴化氢分离重金属; (e)分析在步骤(d)中分离出的重金属。根据本发明,通过重矿物的同位素分析来分析土壤和河流沉积物的重金属污染源的方法具有更准确地分析重金属污染源的人工来源和自然来源的优点。通过分离并获得受污染的土壤和河流沉积物中的重矿物质并进行同位素分析来获得铅。

著录项

  • 公开/公告号KR101824869B1

    专利类型

  • 公开/公告日2018-02-02

    原文格式PDF

  • 申请/专利号KR20170097783

  • 发明设计人 LEE PYEONG KOO;

    申请日2017-08-01

  • 分类号G01N1/40;G01N15/04;G01N30/88;G01N33/18;G01N33/20;G01N33/24;

  • 国家 KR

  • 入库时间 2022-08-21 12:38:29

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