PREPARATION AND PROPERTIES OF FLUOROCARBON ALCOHOL 3, 5-DINITROBENZOATES FOR STUDY AS SURFACE ACTIVE AGENTS

摘要

A detailed procedure for the C5 alcohol, which is typical of all of them, is given in the experimental section the most critical reaction variable seems to be temperature. If the reaction temperature is allowed to raise above 35° C, a highly colored product results this color could not be removed completely by recrystallization of the fluorescence of the plate in ultraviolet light or by spraying with 0.5% p-diethylaminobenzaldehyde in 0.25% ethanol hydrogen chloride. There appeared to be some permanent interaction between the esters and the adsorbent wherever a spot was dried.