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NIST-Traceable NMR Method to Determine Quantitative Weight Percentage Purity of Nitrogen Mustard HN-3 Feedstock Samples.

机译：NIsT-可溯源核磁共振法测定氮芥HN-3原料样品的定量重量百分比纯度。

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摘要

A NIST-traceable method for using nuclear magnetic resonance (NMR) with proton detection is described to determine the weight percent purity of feedstock samples containing nitrogen mustard (HN-3).

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作者
McGarvey, D. J.; Creasy, W. R.;
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年度 2013
页码 1-26
总页数 26
原文格式 PDF
正文语种 eng
中图分类工业技术;
关键词
Chemical warfare agents; Nuclear magnetic resonance; Detection; Mustard agents; Nitrogen; Protons; Purity; Sampling; Hn-3; Purity determination; Nitrogen mustard;

机译：化学战剂;核磁共振;检测;芥子气剂;氮;质子;纯度;取样; Hn-3;纯度测定;氮芥;

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专利

1. Comparative toxic effect of nitrogen mustards (HN-1, HN-2, and HN-3) and sulfur mustard on hematological and biochemical variables and their protection by DRDE-07 and its analogues. [J] . Sharma M, Vijayaraghavan R, Agrawal OP International journal of toxicology . 2010,第4期

机译：氮芥（HN-1，HN-2和HN-3）和硫芥子对血液和生化变量的毒性作用及其通过DRDE-07及其类似物的保护作用。
2. Enantiomeric Variability of Distaminolyne A. Refinement of ECD and NMR Methods for Determining Optical Purity of 1-Amino-2-Alkanols [J] . Pearce A. Norrie, Copp Brent R., Molinski Tadeusz F. Molecules . 2019,第1期

机译：Distaminolyne A的对映体变异A.测定1-氨基-2-链烷醇的光学纯度的ECD和NMR方法的细化
3. Using NMR spectroscopic methods to determine enantiomeric purity and assign absolute stereochemistry [J] . Wenzel T.J., Chisholm C.D. Progress in Nuclear Magnetic Resonance Spectroscopy: An International Review Journal . 2011,第1期

机译：使用NMR光谱法确定对映体纯度并指定绝对立体化学
4. Application of intensity estimation method of the FID signal based on the high-order Prony estimation Method and selective evaluation criterion to Purity Estimation in quantitative NMR, dependence of the 13C decoupling and the sample spinning [C] . Nakao Tomoki, Furukawa Toshihiro, Suematsu Takako, International Symposium on Intelligent Signal Processing and Communications Systems . 2014

机译：基于高阶Prony估计方法和选择性评估准则的FID信号强度估计方法在定量NMR纯度估计， 13 C解耦和样品旋转中的应用
5. Optical methods for quantitative analysis of high -purity gallium arsenide, heavily -doped gallium arsenide and aluminum gallium arsenide/gallium arsenide heterojunction devices [D] . Lu, Zhenghao 1993

机译：光学方法定量分析高纯度砷化镓，重掺杂砷化镓和铝砷化镓/砷化镓异质结器件
6. A Novel Method to Assess Bone Marrow Purity is Useful in Determining Blast Percentage by Flow Cytometry in Acute Myeloid Leukemia and Myelodysplasia [O] . AM Aldawood, Z Kinkade, FG Rosado, -1

机译：一种评估骨髓纯度的新方法可用于通过流式细胞术确定急性髓细胞性白血病和骨髓增生异常的高炉百分比。
7. Validation of quantitative nuclear magnetic resonance (QNMR) spectroscopy as a primary ratio analytical method for assessing the purity of organic compounds: a metrological approach [O] . Saed Al-Deen Tareq Chemistry Faculty of Science UNSW 2002

机译：定量核磁共振（QNMR）光谱作为评估有机化合物纯度的主要比率分析方法的验证：一种计量方法
8. NIST-Traceable NMR Method to Determine Quantitative Weight Percentage Purity of Mustard (HD) Feedstock Samples. [R] . McGarvey, D. J., Creasy, W. R., Connell, T. R. 2018

机译：NIsT可溯源核磁共振法测定芥末（HD）原料样品的定量重量百分比纯度。

NIST-Traceable NMR Method to Determine Quantitative Weight Percentage Purity of Nitrogen Mustard HN-3 Feedstock Samples.

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