ZIF‐8 Membrane Separation Performance Tuning by Vapor Phase Ligand Treatment

摘要

Abstract > Vapor phase ligand treatment (VPLT) of 2‐aminobenzimidazole (2abIm) for 2‐methylimidazole (2mIm) in ZIF‐8 membranes prepared by two different methods (LIPS: ligand induced permselectivation and RTD: rapid thermal deposition) results in a notable shift of the molecular level cut‐off to smaller molecules establishing selectivity improvements from ca. 1.8 to 5 for O <sub>2</sub> /N <sub>2</sub> ; 2.2 to 32 for CO <sub>2</sub> /CH <sub>4</sub> ; 2.4 to 24 for CO <sub>2</sub> /N <sub>2</sub> ; 4.8 to 140 for H <sub>2</sub> /CH <sub>4</sub> and 5.2 to 126 for H <sub>2</sub> /N <sub>2</sub> . Stable (based on a one‐week test) oxygen‐selective air separation performance at ambient temperature, 7?bar(a) feed, and 1?bar(a) sweep‐free permeate with a mixture separation factor of 4.5 and oxygen flux of 2.6×10 ?3 ?mol?m ?2 ?s ?1 is established. LIPS and RTD membranes exhibit fast and gradual evolution upon a 2abIm‐VPLT, respectively, reflecting differences in their thickness and microstructure. Functional reversibility is demonstrated by showing that the original permeation properties of the VPLT‐LIPS membranes can be recovered upon 2mIm‐VPLT. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 通过两种不同的方法（嘴唇：配体诱导的渗滤和RTD：快速热沉积）制备的ZIF-8膜中的2-甲基咪唑（2mim）的2-甲基咪唑（2mIM）的ZIF-8膜（2mmim）的蒸汽相配体（2mim）。结果分子水平截止至较小分子建立从CA的选择性改进。 1.8至5 o <sub> 2 </ sub> / N. <sub> 2 </ sub> ; 2.2至32合作 <sub> 2 </ sub> / ch. <sub> 4 </ sub> ; 2.4至24款 <sub> 2 </ sub> / N. <sub> 2 </ sub> ; 4.8至140 <sub> 2 </ sub> / ch. <sub> 4 </ sub> 和5.2到126 <sub> 2 </ sub> / N. <sub> 2 </ sub> 。稳定（基于一周试验）氧选择性空气分离性能在环境温度下，7？棒（a）饲料，1°（a）扫描（a）的扫描渗透物，其混合物分离因子为4.5和氧气通量2.6×10 ？3 </ sup> ？mol？m ？2 </ sup> ？S. ？1 </ sup> 成立。唇疱和RTD膜分别在2abim-VPLT上表现出快速和逐渐发展，反映其厚度和微观结构的差异。通过表明可以在2mIM-VPLT上回收VPLT-唇膜的原始渗透性能来证明功能性可逆性。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-19011/'>《Angewandte Chemie》</a> <b style="margin: 0 2px;">|</b><span>2019年第46期</span><b style="margin: 0 2px;">|</b><span>共5页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1188.html" title="应用化学">应用化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ligand-induced permselectivity&option=203" rel="nofollow">ligand-induced permselectivity;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=membranes&option=203" rel="nofollow">membranes;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=metal–organic frameworks&option=203" rel="nofollow">metal–organic frameworks;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=vapor phase&option=203" rel="nofollow">vapor phase;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ZIF-8&option=203" rel="nofollow">ZIF-8;</a> </p> <div class="translation"> 机译：配体诱导的偏移;膜;金属 - 有机框架;气相;ZIF-8; 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