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首页> 外文期刊>Angewandte Chemie >Vacancy Engineering of Iron‐Doped W18O49 Nanoreactors for Low‐Barrier Electrochemical Nitrogen Reduction
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Vacancy Engineering of Iron‐Doped W18O49 Nanoreactors for Low‐Barrier Electrochemical Nitrogen Reduction

机译：用于低阻隔电化学氮的铁掺杂W18O49纳米反应器的空位工程

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Abstract > The electrochemical nitrogen reduction reaction (NRR) is a promising energy‐efficient and low‐emission alternative to the traditional Haber–Bosch process. Usually, the competing hydrogen evolution reaction (HER) and the reaction barrier of ambient electrochemical NRR are significant challenges, making a simultaneous high NH <sub>3</sub> formation rate and high Faradic efficiency (FE) difficult. To give effective NRR electrocatalysis and suppressed HER, the surface atomic structure of W <sub>18</sub> O <sub>49</sub> , which has exposed active W sites and weak binding for H <sub>2</sub> , is doped with Fe. A high NH <sub>3</sub> formation rate of 24.7?μg?h ?1 ?mg <sub>cat</sub> ?1 and a high FE of 20.0?% are achieved at an overpotential of only ?0.15?V versus the reversible hydrogen electrode. Ab?initio calculations reveal an intercalation‐type doping of Fe atoms in the tunnels of the W <sub>18</sub> O <sub>49</sub> crystal structure, which increases the oxygen vacancies and exposes more W active sites, optimizes the nitrogen adsorption energy, and facilitates the electrocatalytic NRR. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 电化学氮还原反应（NRR）是传统Haber-Bosch工艺的有希望的节能和低排放替代品。通常，竞争的氢气进化反应（她）和环境电化学NRR的反应屏障是显着的挑战，同时高NH <sub> 3 </ sub> 形成率和高法拉效率（FE）困难。为了给予效率的NRR电催化并抑制她的表面原子结构 <sub> 18 </ sub> O. <sub> 49 </ sub> ，它暴露了活性W网站，对H弱结合 <sub> 2 </ sub> ，掺杂有Fe。高NH. <sub> 3 </ sub> 形成率为24.7？μg？h ？1 </ sup> ？米格 <sub> cat </ sub> ？1 </ sup> 并且在仅α0.15ΩV的过电位与可逆氢电极的过电位，实现了20.0倍的高Fe。 AB？Initio计算揭示了W的隧道中Fe原子的插入式掺杂 <sub> 18 </ sub> O. <sub> 49 </ sub> 晶体结构增加氧空位并暴露更多W活性部位，优化氮吸附能量，并促进电催化NRR。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-19011/'>《Angewandte Chemie》</a> <b style="margin: 0 2px;">|</b><span>2020年第19期</span><b style="margin: 0 2px;">|</b><span>共6页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Tong Yueyu&option=202" target="_blank" rel="nofollow">Tong Yueyu;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Guo Haipeng&option=202" target="_blank" rel="nofollow">Guo Haipeng;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liu Daolan&option=202" target="_blank" rel="nofollow">Liu Daolan;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yan Xiao&option=202" target="_blank" rel="nofollow">Yan Xiao;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Su Panpan&option=202" target="_blank" rel="nofollow">Su Panpan;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liang Ji&option=202" target="_blank" rel="nofollow">Liang Ji;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhou Si&option=202" target="_blank" rel="nofollow">Zhou Si;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liu Jian&option=202" target="_blank" rel="nofollow">Liu Jian;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Lu Gao Qing (Max)&option=202" target="_blank" rel="nofollow">Lu Gao Qing (Max);</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Dou Shi Xue&option=202" target="_blank" rel="nofollow">Dou Shi Xue;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Institute for Superconducting &</p> <p>Electronic MaterialsUniversity of WollongongNorth Wollongong NSW 2500 Australia;</p> <p>Institute for Superconducting &</p> <p>Electronic MaterialsUniversity of WollongongNorth Wollongong NSW 2500 Australia;</p> <p>Institute for Superconducting &</p> <p>Electronic MaterialsUniversity of WollongongNorth Wollongong NSW 2500 Australia;</p> <p>Institute for Superconducting &</p> <p>Electronic MaterialsUniversity of WollongongNorth Wollongong NSW 2500 Australia;</p> <p>State Key Laboratory of CatalysisChinese Academy of Sciences457 Zhongshan Road Dalian 116023 P. R. China;</p> <p>Institute for Superconducting &</p> <p>Electronic MaterialsUniversity of WollongongNorth Wollongong NSW 2500 Australia;</p> <p>Institute for Superconducting &</p> <p>Electronic MaterialsUniversity of WollongongNorth Wollongong NSW 2500 Australia;</p> <p>State Key Laboratory of CatalysisChinese Academy of Sciences457 Zhongshan Road Dalian 116023 P. R. China;</p> <p>DICP-Surrey Joint Centre for Future MaterialsUniversity of SurreyGuilford Surrey GU2 7XH UK;</p> <p>Institute for Superconducting &</p> <p>Electronic MaterialsUniversity of WollongongNorth Wollongong NSW 2500 Australia;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1188.html" title="应用化学">应用化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=electrocatalysts&option=203" rel="nofollow">electrocatalysts;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=nanoreactor&option=203" rel="nofollow">nanoreactor;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=nitrogen reduction reaction&option=203" rel="nofollow">nitrogen reduction reaction;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=tungsten oxide&option=203" rel="nofollow">tungsten oxide;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=vacancy engineering&option=203" rel="nofollow">vacancy engineering;</a> </p> <div class="translation"> 机译：电催化剂;纳米反应器;氮气还原反应;氧化钨;空缺工程; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704028161980.html">Back Cover: Vacancy Engineering of Iron‐Doped W18O49 Nanoreactors for Low‐Barrier Electrochemical Nitrogen Reduction (Angew. 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