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Well-designed β-Ag_2MoO_4 crystals with photocatalytic and antibacterial activity

机译:精心设计的具有光催化和抗菌活性的β-Ag_2MoO_4晶体

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This paper describes the beta silver molybdate (beta-Ag2MoO4) samples with spinel-type cubic structures synthesized with various morphologies, including round tips coral-like, elongated coral-like and truncated cube, by themicrowave-assisted solvo-/hydrothermal method. The crystalmorphologies could be controlled by adjusting the solvent, surfactant, and pH of the precursor solution. X-ray diffraction, field-emission scanning electron microscopy, Fourier-transform Raman spectroscopy, and diffuse reflectance spectroscopy in the ultraviolet-visible (UV-Vis) region, were used to characterize the structures of the samples. The specific surface area was determined using the Brunauer-Emmett-Teller method. Furthermore, the photocatalytic/antibacterial properties of the particles were dependent on the beta-Ag2MoO4 crystal morphogy and were evaluated by Rhodamine B dye photodegradation under UV-Vis light, and by determining their minimuminhibitory and bactericidal concentrations, using a broth microdilution assay for Escherichia coli bacteria. (C) 2016 Elsevier Ltd. All rights reserved.
机译:本文介绍了用微波辅助溶剂-水热法合成的尖晶石型立方结构的β-钼酸银(β-Ag2MoO4)样品,具有多种形态,包括圆头珊瑚状,细长的珊瑚状和截短的立方体。可以通过调节前体溶液的溶剂,表面活性剂和pH值来控制其晶体形态。使用X射线衍射,场发射扫描电子显微镜,傅立叶变换拉曼光谱和紫外可见(UV-Vis)区域的漫反射光谱来表征样品的结构。使用Brunauer-Emmett-Teller方法测定比表面积。此外,颗粒的光催化/抗菌性能取决于β-Ag2MoO4晶体的形态,并通过罗丹明B染料在紫外-可见光下的光降解,并通过使用肉汤微量稀释法测定大肠杆菌的最小抑菌和杀菌浓度来进行评估。菌。 (C)2016 Elsevier Ltd.保留所有权利。

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