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Preparation and Characterization of ZnO and Mg-ZnO nanoparticle

机译:ZnO和Mg-ZnO纳米粒子的制备与表征

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摘要

ZnO is one of the most promising materials since it has a high mechanical and thermal stability, and wide band gap (3.37 eV). Meanwhile, doping with selective elements offers an effective method to enhance and control the electrical and optical properties of ZnO nanostructures, which is crucial for its practical applications. Mg-doped ZnO have considerable interests owing to their unique optical, electric and piezoelectric properties. In this paper, we report the Synthesis of Mg-doped ZnO nanoparticles successfully with diameters ranging from 50 to 100 nm via precipitation method. The surface morphology of synthesized material was investigated by using scanning electron microscope (SEM) and the elemental analysis by energy-dispersive X-ray spectroscopy (EDAX). The presence of Mg was confirmed by infrared spectroscopic (IR) studies. The structure and phases of Mg-ZnO were analyzed by powder X-ray diffraction (XRD) method and the Optical properties were measured by using UV–Vis spectrophotometer.
机译:ZnO是最有前途的材料之一,因为它具有较高的机械和热稳定性以及较宽的带隙(3.37 eV)。同时,掺杂选择性元素提供了一种有效的方法来增强和控制ZnO纳米结构的电学和光学特性,这对其实际应用至关重要。镁掺杂的氧化锌由于其独特的光学,电学和压电特性而备受关注。在本文中,我们报道了通过沉淀法成功地合成了直径为50至100 nm的Mg掺杂的ZnO纳米颗粒。使用扫描电子显微镜(SEM)研究合成材料的表面形态,并使用能量色散X射线光谱仪(EDAX)研究元素分析。通过红外光谱(IR)研究确认了镁的存在。用粉末X射线衍射(XRD)法分析了Mg-ZnO的结构和相,并用UV-Vis分光光度计测量了光学性能。

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