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Characterizing Complex Mineral Structures in Thin Sections of Geological Samples with a Scanning Hall Effect Microscope

机译:用扫描霍尔效应显微镜表征地质样品薄片中的复杂矿物结构

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摘要

We improved a magnetic scanning microscope for measuring the magnetic properties of minerals in thin sections of geological samples at submillimeter scales. The microscope is comprised of a 200 µm diameter Hall sensor that is located at a distance of 142 µm from the sample; an electromagnet capable of applying up to 500 mT DC magnetic fields to the sample over a 40 mm diameter region; a second Hall sensor arranged in a gradiometric configuration to cancel the background signal applied by the electromagnet and reduce the overall noise in the system; a custom-designed electronics system to bias the sensors and allow adjustments to the background signal cancelation; and a scanning XY stage with micrometer resolution. Our system achieves a spatial resolution of 200 µm with a noise at 6.0 Hz of 300 nTrms/(Hz)1/2 in an unshielded environment. The magnetic moment sensitivity is 1.3 × 10−11 Am2. We successfully measured the representative magnetization of a geological sample using an alternative model that takes the sample geometry into account and identified different micrometric characteristics in the sample slice.
机译:我们改进了磁扫描显微镜,用于在亚毫米尺度上测量地质样品薄片中矿物的磁性。显微镜由直径200 µm的霍尔传感器组成,该霍尔传感器与样品的距离为142 µm。能够在直径40毫米的区域上向样品施加高达500 mT直流磁场的电磁体;第二霍尔传感器以梯度配置布置,以抵消电磁体施加的背景信号并减少系统中的总体噪声;一个定制设计的电子系统,使传感器偏置并允许对背景信号消除进行调整;和具有微米分辨率的扫描XY平台。在非屏蔽环境中,我们的系统可实现200 µm的空间分辨率,在6.0 Hz处的噪声为300 nTrms /(Hz) 1/2 。磁矩灵敏度为1.3×10 −11 Am 2 。我们使用替代模型成功地测量了地质样品的代表性磁化强度,该模型考虑了样品几何形状并确定了样品切片中的不同微米特征。

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