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高频红外分析法同时测定煤中碳和硫

         

摘要

报道了高频红外分析仪同时测定煤中碳和硫的方法,可测w(C)为0%~80%,w(S)为0%~2.0%。方法经国家一级标准物质分析验证,结果与标准值相符,相对标准偏差(RSD,n=8)C<1.7%,S<1.3%。%A method for simultaneous determination of carbon and sulfur in coal samples by HFIR C/S analyzer is described in this paper. The proposed method provides a wide concentration range for carbon (w=0%~80%) and sulfur (w=0%~2%). The method has been verified by the determination of carbon and sulfur in standard reference coal samples. The results are in agreement with certified values with precision (n=8) of<1.7% RSD for carbon and <1.3% RSD for sulfur.

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