CRYSTAL AND MOLECULAR STRUCTURE OF PALMATINE CHLORIDE PHENOL SOLVATE MONOHYDRATE

摘要

＜正＞ The crystal of palnatine chloride phenol solVate monohydrate belongs to the triclinic, space group Cl-P1 with the unit cell parameters of a =14.781, b=11.246, c= 7.505 A,α=95.26（7）°,β=96.87（4）°,γ=94.32（4）°,and Z=2,The coordinates for all the non-hydrogen atoms were found by using direct methods and Sim weighting Fourier synthesis. The anisotropic refinement of non-hydrogen atoms and isotropic refinement of hydrogen atoms led to a final R-factor of 0.055. Solvate molecules form a relatively complex network around chloride ion.In this paper palmatine nolecule structure and the network of solvent molecules are described.