CRYSTAL AND MOLECULAR STRUCTURE OF BIS（O,O’-DICYCLOHEXYLDITHIOPHOSPHATO）-NICKEL（Ⅱ）

摘要

＜正＞ Ni[（C6H11O）2PS2]2, Mr=627.39, Monoclinic, P21/n, a=11.802（7）, b= 9.336（2）, c=14.177（5） A,B=96.72（4）°,V=1551.3A3, Z=2, Dc=1.343g·cm-3, MoKα radiation λ=0.71073A, F（000）=648e, R=0.068 for 2642 reflections. Ni（Ⅱ） atom is surrounded by four sulfur atoms, forming a square.