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Synthesis of hydroxyapatite assisted by surfactants

机译:表面活性剂辅助合成羟基磷灰石

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Hydroxyapatite (HAp) nanoparticles were synthesized with cationic surfactant, anionic surfactant and nonionic surfactant tuwen 80 respectively. The products were characterized by transmission electronmicroscopy (TEM), X-ray diffraction (XRD), and fourier transform infrared (FTIR) spectroscopy. The results show the characteristic peaks of HAp with size between 75–100 nm, which indicate the successful preparation of HAp nanoparticles. The images of TEM display the needle-like structure of HAp crystals by adding cationic surfactant, however rectangular structure of HAp crystals is obtained by adding anionic surfactant. It revealed that the morphology of HAp could be adjusted by surfactants, which might provide a new way of preparing HAp nanoparticles with controllable morphology.
机译:分别用阳离子表面活性剂,阴离子表面活性剂和非离子表面活性剂土文80合成了羟基磷灰石(HAp)纳米颗粒。产品通过透射电子显微镜(TEM),X射线衍射(XRD)和傅立叶变换红外(FTIR)光谱进行了表征。结果表明,HAp的特征峰尺寸在75–100 nm之间,这表明成功制备了HAp纳米颗粒。 TEM图像通过添加阳离子表面活性剂显示出HAp晶体的针状结构,但是通过添加阴离子表面活性剂获得了HAp晶体的矩形结构。结果表明,表面活性剂可以调节HAp的形貌,为制备具有可控形态的HAp纳米颗粒提供了新途径。

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