首页> 外文会议>International Conference on Textures of Materials;ICOTOM 15 >EFFECT OF TIN ON THE RECRYSTALLIZATION BEHAVIOR AND TEXTURE OF GRAIN ORIENTED ELECTRICAL STEELS
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EFFECT OF TIN ON THE RECRYSTALLIZATION BEHAVIOR AND TEXTURE OF GRAIN ORIENTED ELECTRICAL STEELS

机译:锡对晶粒取向钢的再结晶行为和织构的影响

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Influence of tin, range from 0 - 0.31wt%, on the recrystallization behavior and texture of grain oriented electrical has been investigated. Tin is susceptible to segregation at grain boundary and on surface that pinning down the grain boundary mobility. Annealed hot bands in 2.5mm are cold rolled to 0.35 mm in one-stage cold rolling. Cold-rolled sheets are decarburization annealing at 800°C for 5 minutes in wet H_2-N_2 atmosphere. During secondary recrystallization specimens are heated to 900 ~1200 °C and soaked 12 hours with a heating rate 12 °C per hour after 700 °C. Both X-ray and EBSD are conducted to examine the grain orientation.It is found that pinning effect of tin is very strong for secondary recrystallization. The specimens containing less than 0.05wt% tin finish secondary recrystallization after SRT at 1000 °C. The secondary recrystallization grain growth became difficult as the tin content above 0.10wt%. According to EBSD results, after primary recrystallization, the intensity of (011)<001> texture in the specimens with nitriding 30 seconds slightly increases with increasing tin content and reaches a maximum value at 0.05wt% tin. Then, it rapidly decreases with increasing tin and reaches a minimum at 0,21wt% tin. Finally, it increases with increasing tin again. However, the intensity of (011)<001> texture in the specimens without nitriding decreases with increasing tin content and reaches a minimum value at 0.21 wt% tin. Then, it increases with increasing tin. Both EBSD and XRD results show that the intensities of (111) textures in the specimens both with and without nitriding decreases with increasing tin content and reaches a value at 0.05 wt% tin. Then, it increases with increasing tin and reaches a peak at 0.1 wt% tin. Finally, it decreases with increasing tin again. For the specimens without nitriding treatment, while the SRT is higher than 1100 °C, best magnetic properties was occurred in the steel containing 0.05 wt% tin. However, the flux density increases and core loss decreases with increasing the tin content after nitriding and secondary annealing at 1000 °C. Nitriding can improve the magnetic properties of grain oriented electrical steels.
机译:研究了锡含量在0-0.31wt%范围内对晶粒取向电子的再结晶行为和织构的影响。锡易于在晶界和表面偏析,从而限制了晶界的迁移率。 2.5毫米的退火热轧带在一级冷轧中被冷轧至0.35毫米。将冷轧板在潮湿的H_2-N_2气氛中于800°C进行5分钟的脱碳退火。在二次重结晶过程中,将样品加热到900〜1200°C,并在700°C之后以每小时12°C的加热速率浸泡12小时。进行X射线和EBSD检查晶粒取向。 发现锡的钉扎作用对于二次重结晶非常强。锡含量低于0.05wt%的样品在1000°C下进行SRT后完成二次重结晶。当锡含量超过0.10wt%时,二次重结晶晶粒的生长变得困难。根据EBSD结果,在初次重结晶后,渗氮30秒的样品中(011)<001>织构的强度随锡含量的增加而略微增加,并在锡的0.05wt%时达到最大值。然后,它随着锡的增加而迅速下降,并在锡的0.21%(重量)时达到最小值。最后,它随着锡的增加而增加。但是,没有氮化的样品中的(011)<001>织构强度随锡含量的增加而降低,并在0.21 wt%的锡时达到最小值。然后,它随着锡的增加而增加。 EBSD和XRD结果均表明,在有和没有氮化的情况下,样品中的(111)uvw织构强度随锡含量的增加而降低,并达到0.05重量%锡的值。然后,它随着锡的增加而增加,并在锡的0.1 wt%处达到峰值。最后,它随着锡的增加而减少。对于未经氮化处理的样品,当SRT高于1100°C时,在含0.05 wt%锡的钢中表现出最佳的磁性能。但是,在1000°C氮化和二次退火后,随着锡含量的增加,磁通密度增加,铁损降低。渗氮可以改善晶粒取向电工钢的磁性能。

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